By James Blake Rawlings
This can be a chemical engineering textbook for undergraduate and graduate scholars in reactor layout and response engineering classes.
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However, utmost care must be taken and the repeatability and reproducibility of adsorption and desorption isotherms for relatively well-understood materials should be thoroughly tested to confirm that a sufficiently pure hydrogen supply configuration has been achieved. Impurity levels in other gases should also be considered, however, because impurities can potentially block the adsorption of any adsorptive species. This is particularly relevant in the case of microporous solids because the strong adsorption potentials of the small pores are more likely to attract impurities.
3). However, the accuracy with which the degassed sample mass can be determined is Potential Error Sources also important. The measurement of sample sizes lower than 50 mg, for example, on a typical laboratory balance may contain a significant error. In gravimetric systems, this is less of an issue for small samples because the instrument typically incorporates a highly sensitive and accurate microbalance that can measure accurate sample weights of less than a milligram. An appropriate sample size choice in each technique is also highly dependent on the adsorption capabilities of the material in question.
62, 1573–1659. 57. , Baker, R. T. , and Rodriguez, N. M. (1998). Hydrogen storage in graphite nanofibers, J. Phys. Chem. B, 102(22), 4253–4256. 58. , and Steriotis, T. (2009). A Round Robin characterisation of the hydrogen sorption properties of a carbon based material, Int. J. Hydr. , 34(7), 3044–3057. 37 38 Techniques for the Measurement of Gas Adsorption by Carbon Nanostructures 59. , and Seaton, N. A. (2009). Characterisation of Porous Solids VIII: Proceedings of the 8th International Symposium on the Characterisation of Porous Solids, eds.
Chemical Reactor Analysis and Design Fundamentals - Rawlings by James Blake Rawlings